QUÁ TRÌNH THIÊU KẾT PHA RẮN

Quá trình thiêu kết pha rắn được thực hiện bằng cách dịch chuyển vật chất trong pha rắn dưới tác dụng của nhiệt độ. Chuỗi các quá trình xảy ra trong quá trình thiêu kết pha rắn có thể được chia, theo đặc điểm hình học thuần túy, thành ba giai đoạn.

Giai đoạn thiêu kết ban đầu.

Ở giai đoạn này, độ xốp của phôi ép rất cao, và độ nén của thân hạt trước tiên xảy ra do sự trượt của các hạt dọc theo ranh giới hạt. Do đó, giai đoạn đầu tiên của quá trình nén có liên quan đến sự chuyển động của các hạt nói chung. Chuyển động này kết thúc khi đạt được một vật thể xít chặt. Ở giai đoạn này, sự thiêu kết lẫn nhau của các hạt cũng xảy ra. Nó đi kèm với sự gia tăng trong khu vực tiếp xúc giữa chúng.

Giai đoạn trung gian

Giai đoạn này được đặc trưng bởi các điểm tiếp xúc giữa các hạt đang nhanh chóng mở rộng. Các hạt dần dần hợp nhất với nhau, mất đi tính cá nhân. Trong giai đoạn này, vật thể thiêu kết có thể được biểu diễn dưới dạng kết hợp của hai pha xen kẽ ngẫu nhiên – pha rắn và pha rỗng (chân không). Các lỗ trống (là phần không gian trống trong vật thể) ban đầu có được ở dạng của các kênh kết nối (lỗ trống hở – mở). Quá trình điền đầy ở giai đoạn thiêu kết này không liên quan đến sự chuyển động của từng hạt, nhưng được thực hiện bằng cách dịch chuyển khốilượng trong thể tích vật chất và theo bề mặt của các hạt.

Ranh giới tiếp xúc giữa các hạt bị nung tạo thành một cầu nối có bề mặt lõm và bán kính cong nhỏ. Nồng độ của lỗ trống (một dạng khuyết tật của mạng tinh thể) ở gần bề mặt (mặt lõm) này lớn hơn gần bề mặt lồi của hạt. Do đó, các lỗ trống khuếch tán từ cầu nối đến bề mặt của các hạt và bị kết thúc ở đó. Bằng cách nhảy tương tự khuếch tán dòng chảy của các hạt vật chất, mở rộng nó, dần dần lấp đầy lỗ rỗng. Do một phần dòng chảy của một chất hướng vào bề mặt của cây cầu được đưa đến các khu vực tiếp xúc giữa các hạt, các hạt tiếp cận nhau, nghĩa là vật liệu co lại.

Giai đoạn cuối cùng của thiêu kết.

Ở giai đoạn này, trong một vật thể thiêu kết, hầu hết chỉ có lỗ rỗng khép kín, bị cô lập. Trong quá trình thiêu kết, số lượng và kích thước của chúng (lỗ rỗng khép kín) giảm dần do sự phát triển quá mức (quá trình điền đầy vật chất). Cơ chế phát triển quá mức như vậy về cơ bản giống như ở giai đoạn thiêu kết trung gian. Ví dụ, xem xét một lỗ rỗng bị cô lập trong hạt. Bán kính của lỗ rỗng này nhỏ hơn nhiều so với bán kính của hạt, vì nồng độ của chỗ trống gần bề mặt cong của lỗ rỗng có độ cong lớn sẽ cao hơn bề mặt của hạt có độ cong thấp hơn. Do đó, lỗ trống sẽ di chuyển từ lỗ rỗng đến bề mặt của hạt. Các nguyên tử hoặc ion di chuyển theo hướng ngược lại, tức là, đến bề mặt lỗ rỗng, và lấp đầy nó.

Theo một số dữ liệu, cơ chế hòa tan chỗ trống của lỗ rỗng được quan sát thấy nếu kích thước lỗ rỗng nhỏ hơn đáng kể so với kích thước hạt. Cơ chế của dòng chảy nhớt có thể hoạt động ở tỷ lệ nghịch, tức là khi một lỗ rỗng lớn được bao quanh bởi các hạt nhỏ.

 

 

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  • KneentyfubWeeme
  • seerveproto
  • Fumsmubysap
  • ERANNINOINHAW
  • Heitoentfeftota
  • EluttjallesCasp
  • StesmymnHoose
  • effequatt
  • MelogroowlPep
  • Bupemettyimmets
  • algoriasase
  • spillicietbap