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Ép nguội không cung cấp độ bền cơ học cho phôi ép, và chúng có thể bị phá vỡ ngay cả với một tác động nhỏ. Để cải thiện các tính chất cơ học và tạo cho các sản phẩm tính chất lý hóa cần thiết của phôi, chúng phải được thiêu kết.

Thiêu kết vật liệu bột – là gia công nhiệt của bột, ở trạng thái rắc tự do hoặc phôi ép ở nhiệt độ từ 0,7 đến 0,9 nhiệt độ nóng chảy tuyệt đối của bột kim loại trong hệ một thành phần hoặc thấp hơn nhiệt độ nóng chảy của bột kim loại chính trong hệ đa thành phần. Thiêu kết của bất kỳ hệ thống nào đều bao gồm sự nung nóng các sản phẩm đến một nhiệt độ định trước, nhiệt hóa đẳng nhiệt ở nhiệt độ này và làm mát đến nhiệt độ phòng.

Trong quá trình thiêu kết vật liệu bột, các loại khí và sự hấp thụ trên bề mặt các hạt được loại bỏ, sự bay hơi của các tạp chất khác nhau, loại bỏ các ứng suất còn lại trong các vùng tiếp xúc giữa các hạt và của bản thân các hạt, giảm màng oxit, hòa tan hoặc đông tụ, sắp xếp lại lớp bề mặt, kết quả của sự khuếch tán và dịch chuyển kim loại ở dạng hơi từ nơi này đến nơi khác, kết tinh lại, v.v.

Các quá trình quan trọng trong thiêu kết là những thay đổi định tính và định lượng của sự tiếp xúc giữa các hạt. Sự tiếp xúc giữa các hạt từ oxit trong nền được chuyển biến thành dạng kim loại, và nó phát triển, tỷ lệ giữa các lỗ trống và thể tích của kim loại làm giảm thể tích của các lỗ trống.

Trong luyện kim, thuật ngữ “thiêu kết” được hiểu là một trong những hoạt động công nghệ quan trọng nhất của luyện kim bột, trong đó, kết quả của sự khuếch tán, tái kết tinh và các quá trình khác trong quá trình xử lý nhiệt một chi tiết được tạo ra với một cấu trúc và đặc tính nhất định từ phôi rắc bột tự do hoặc phôi ép.

Từ quan điểm của hóa lý chất rắn, thiêu kết đã được trình bày. Một quá trình động học tự phát nhiều giai đoạn phức tạp mang một tập hợp các hạt gần với trạng thái cân bằng nhiệt động lực học.

Sự không cân bằng nhiệt động lực học của bột là do sự phát triển mạnh mẽ của bề mặt tự do của các hạt, sự hiện diện của biến dạng siêu nhỏ của cấu trúc tinh thể của các hạt kim loại (micropores, dislocations, vacancies, defections, vv) và sự không hoàn hảo của sự tiếp xúc giữa chúng, và trong trường hợp hỗn hợp bột của nhiều thành phần khác nhau, còn do sự phân bố không đồng đều của các thành phần hạt.

Do đó, bất kỳ phôi ép nào đều có một năng lượng dư lớn, đó là động lực chính của quá trình thiêu kết. Về mặt này, từ quan điểm nhiệt động lực học, quá trình thiêu kết có thể được xem như một quá trình khôi phục cấu trúc nguyên tử tinh thể của một hạt kim loại, cũng như quá trình di chuyển các nguyên tử từ những nơi “không thuận lợi” đến những nơi năng lượng tự do của hệ thống ở mức nhỏ nhất. Nói cách khác, quá trình thiêu kết là quá trình động học giải phóng hệ thống bột khỏi các khuyết tật không cân bằng.

Một trong những biểu hiện đặc trưng nhất của quá trình thiêu kết là giảm kích thước – “co ngót” của sản phẩm, kèm theo việc “chữa lành” các khuyết tật trong cấu trúc tinh thể kim loại của các hạt.

Sự đa dạng của các khuyết tật vi mô và vĩ mô trong phôi ép chưa thiêu kết sẽ xác định sự đa dạng của các cơ chế “chữa bệnh” của chúng. Kết quả là, trong quá trình thiêu kết, các quá trình động học phân tử quan trọng nhất là các phản ứng hóa học ở bề mặt và ở các biên giới hạt, sự khuếch tán bề mặt và thể tích, và các quá trình phân tán kích hoạt nhiệt.

Việc thiết lập các quy luật lý thuyết của quá trình thiêu kết là chủ đề của một số lượng lớn các công trình nghiên cứu của các nhà khoa học, cho phép xây dựng lý thuyết hiện đại và giải thích các quá trình xảy ra trong quá trình thiêu kết kim loại bột và hợp kim.

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